Step 24. Nitride removal                          

 

Images taken by uvscope after the nitride removal:  STI        LOCOS

 

 

Step

 

Process

Date

Operator

24.1

 

 

Oxide wet etch

 

Sink 6

1/10 HF dip for 60 s

Etch thin oxide layer off from the top of the nitride film.

Include PCH.

 

08/16/07

  Pongracz

24.2

 

 

Sink7

-         fresh phosphoric acid (3 bottles) @ 160 oC

-         water dripping 1 drop/10s to keep the liquid level

-         monitor the etch rate (QDR, SRD)

-         measure oxide/nitride thickness with Nanoduv

 

LOCOS wafers W#1-5 and 11-15 and PCH

90min etch monitor nitride thickness after 30min, 45 min, 65 min, 80 min

After 80 min oxide thickness is 216 A

Allow 10 min more etching

 

STI wafers W#6-10

125 min etch monitor nitride thickness after 30min, 60 min, 90 min, 105 min

After 105 min nitride is still there on some places

Allow 20 min more etching

 

 

Nitride remained on some spots very close to the edge because of CMP non-uniformity

 

08/16/07-

08/17/07

 

24.3

 

 

Pad oxide wet etch

 

1/10 HF @ Sink6 until PCH dewet ~ 60 s

 

 

08/17/07

24.4

 

Oxide wet etch from NCH

 

5:1 BHF @ Sink8 until dewet ~ 5 min

 

 

08/17/07