Chapter 2.7

Sink7 (VLSI)

(sink7)

1.0         Title

Sink7 in the VLSI area

 

2.0         Purpose

This document has specific information about wet sink7, Microlab’s MOS and Non-MOS 6” sink.

 

3.0         Scope

Wet Sink7 provides a Big Batch silicon etch bath, a hot phosphoric acid bath, and two HF tanks as well as two DI water rinse followed by a quick dump. Each chemical bath and/or tank is clearly labeled.

4.0         Applicable Documents

Revision History

4.1         Heated Phosphoric Acid Etching of Silicon Nitride - Concentration and Temperature Control

4.2         Chapter 2.3 of the lab manual (Wet Sinks and Spin Dryers)

4.3         Chapter 2.1 of the lab manual, which explains wafer boxes, tweezers, and other tool cleaning prior to using VLSI sink.

5.0         Definitions & Process Terminology

5.1         Full Plenum Lockout Alarm: Early warning alarm indicating sink drain failure.

5.2         Quick dump rinse (QDR): DI water fills the sink followed by a quick dump to get ride of excess acid and/or contaminants.

5.3         Spin Rinse Dryer (SRD): DI rinse followed by dry cycle.

6.0         Safety

Never touch any surface while wearing chemical-resistant gloves that other lab members may come into contact with, such as the table tops, door handles, computer keyboards, face shields, aprons, etc. If you need to step away from the sink at any time, rinse off gloves at the glove wash, dry with techni-cloths, and put away in your drawer until you are ready to resume your work at the sink.

Follow general safety guidelines for the lab safety rules outlined in Chapter 2.3 and the following:

6.1         This sink contains a Big Batch silicon etch bath, a hot phosphoric acid bath, and two HF tanks; therefore appropriate safety attire should be worn while working at this station. This means that chemically resistant gloves on top of the surgical gloves, face shield, and apron have to be worn while working at or around sink7. Do not use metal tweezers at this sink.

6.2         Do not adjust the heater controllers as they have been preset to produce proper bath temperatures.

6.3         Only use chemically resistance cassettes provided at the station (Teflon type). Failure to do so can cause damage to the station and/or compromise the operator’s safety.

6.4         Dwyer Photohelic Exhaust Flow Meter (Figure 5): Monitors the sink exhaust flow and will shut down all electricity and water to the sink if there is too much or too little flow. An alarm will sound; press the red SILENCE button (Figure 4) and promptly report on FAULTS.

6.5         MPC-901 Emergency Alarm (Figure 4): Cuts power to the sink in emergencies. Push the big red STOP button (Figure 4) to cut the power to this sink. Report promptly on FAULTS.

6.6         Glove Wash: Located in the front center of this sink; water spray is sensor activated.

7.0         Statistical/Process Data

N/A

8.0         Available Processes, Gases, Process

Big Batch silicon etch bath, hot phosphoric acid bath, and two drainable HF tanks are available at this sink as well as two quick dump rinsers to properly clean the wafers prior to going into the 6” spin rinse dryer (top SRD on the rack.)

 

Bath

Chemical

Temperature

Left-Heated Bath

Big Batch Silicon Etch

60ºC

Right-Heated Bath

Hot Phosphoric Acid

160ºC

Left Non-Heated Tank

Non-MOS clean HF

N/A

Right Non-Heated Tank

MOS-clean HF

N/A

 

9.0         Equipment Operation

The sink operation is relatively easy. The main difference between the old and new style VLSI sinks is that at the new sinks members invoke the dump rinse cycle from a keypad mounted on the face of the station (one for each quick dump rinse tank).

9.1         Control Key Description

There are six control/displays at this station, see Figures & Schematics. The two MPC-100 (Figure 3) control panels are for the heated baths: the one on the left is for the Big Batch silicon etch, the one on the right for the hot phosphoric bath. The two MICROKLEEN RINSE (Figure 1) control panels are for the two quick dump rinse (QDR) stations. Each QDR is currently set up for two dump rinse cycles. Wafers are initially showered with DI water followed by two DI fill-dump cycles. These cycles end with wafers submerged in the water for operator to extract and place them in SRD. See Figures & Schematics for more details. The station performs an automatic self-cleaning, every 60 minutes by one QDR cycle. The MICROTIMER (Figure 2) control panel timers for the HF baths are preset to 15 minutes.

POWER            Turns on the control panel.

START             Begins a process cycle at any of the control/display panels.

STOP/RESET    Stops or interrupts a process cycle at any time.

SAVE/SIL         Silences the acid bath alarm.

HOLD               Stops heating the Big Batch silicon etch or hot phosphoric acid bath corresponding to the control/ display panels. Press HOLD again or RETURN to reactivate the heater.

DRAIN              Press twice to empty the baths/tanks. Make sure chemicals baths are sufficiently cooled down before draining. To only drain a small amount, press the DRAIN button twice, then once again when you want to stop the draining.

9.2     Quick Dump Rinse Operation

9.2.1          Place wafers in the tank; tank initially should be full of DI water.

9.2.2          Press START button to activate the dump rinse cycle (Figure 1). It will cycle down from 2 to 1 then show 0 in the display window. At the end of the two cycles a beeping alarm will sound. Press STOP/RESET to silence the alarm. Upon completion of two rinse cycles remove wafers and place in SRD.

9.2.3          Note: Dump the QDR water by pressing the OPEN button. This will open the gate at the bottom of the sink to drain the water. Press STOP/RESET to close the gate after the water is drained. Leave the QDR with no water in it and with closed lid, before leaving the station.

9.3     Room Temperature HF Controllers (Microtimer Operation)

9.3.1     Place your wafers in the desired HF acid bath (left bath is designated non-MOS clean, right bath is designated MOS-clean).

9.3.2     Press the START button if you wish to use the 15-minute preset timer; use of this is optional (Figure 2).

9.3.3          Press STOP/RESET button to end or interrupt the cycle.

9.3.4          To reset the timer at end of cycle, press STOP/RESET once again.

9.3.5          Remove wafers and rinse in either of the quick dump rinsers.

 9.4    Hot Bath Controller for Big Batch Silicon or Hot Phosphoric Bath (MPC-100)

9.4.1     Place your wafers in desired bath, either the Big Batch silicon etch (staff use only) or the hot phosphoric bath.

9.4.2     Press time/start button to start the etch process cycle with the preset time and temperature (Figure 3).

9.4.3     When your etch is completed after the preset time, hit the TIME STOP/RESET button to reset the timer.

9.4.4          Remove your wafers and rinse in quick dump rinse #1 for the Big Batch silicon etch or quick dump rinse #2 for the hot phosphoric.

9.5         Changing Acid(s) in Sink7

9.5.1          Big Batch Silicon Etch (Figure 3):

9.5.1.1    Press the HOLD button once on the MPC-100 temperature controller panel so that the bath temperature will cool down to 60ºC. Note: LED light next to Heat, under status column, goes off.

9.5.1.2    Next, press the DRAIN button twice to empty the bath. Rinse bath with DI water after completely drained. The timer is set for 10 minutes. Do not put solution in bath before this time has elapsed.

9.5.1.3    Press DRAIN button again to close the gate on the bottom of the tank. Fill the bath with new Big Batch silicon etch.

9.5.1.4    Press HOLD button to restart the heater. LED adjacent to Heat, under status column, turns on.

9.5.2          Room Temperature HF Baths (Figure 2):

9.5.2.1    Press the AMBIENT TANK #1/#2 DRAIN green button.

9.5.2.2    Rinse the bath with DI water once the tank is empty.

9.5.2.3    Press the AMBIENT TANK #1/#2 DRAIN green button again.

9.5.2.4    Fill the non-MOS clean or MOS clean HF in the appropriate acid tank accordingly.

9.5.3          Hot Phosphoric Acid Bath (Figure 3):

9.5.3.1    Press the HOLD button on the MPC-100 temperature controller panel so that the bath temperature will cool down to 74.5ºC.

9.5.3.2    Next press the DRAIN button twice to empty the bath. Rinse bath with DI water after completely drained. The drain timer is set for 10 minutes.

9.5.3.3    Press DRAIN button again to close the gate on the bottom of the tank. Fill the bath with new phosphoric acid.

9.5.3.4    Press HOLD button to restart the heater.

9.6         Control Panel Programs are shown in the appendix.

9.6.1          The parameter codes for the programs on the MPC-100 temperature controllers and Microkleen Rinse are listed on Table 1 and Table 2 in the appendix. The parameter codes are not to be altered by the Microlab members. Please use them as your reference check only.

10.0      Troubleshooting Guidelines

10.1      Rinse cycle stopped in the middle QDR cycles: press open to dump the water out. Press stop/reset key followed by restart the dump rinse cycle from the start.

10.2      No Power To Sink: Several issues can shut the system down.

10.2.1      Power To System Off (Figure 4): Press power ON if no issues have been reported on the Wand or if the system is not under technician’s control.

10.2.2      Photohelic Differential Pressure Reading (Figure 5) is outside limits (two red bars): Consult with staff to check house exhaust pressure.

10.2.3      Plenum Full: The plenum on this system is directly connected to fabwide (sink6). Full plenum in sink6 will also stop sink7 operation.

Spin Rinse/Dryer  HElp  Messages

HELP-0

Power Failure

The power failed while the unit was operating. Check the electrical lines in the unit, and for a blown fuse. Press START to reset the microprocessor. The rinser/dryer indexes the rotor and resets to the beginning of the interrupted cycle.

HELP-1

Bladder Pressure

There is inadequate nitrogen pressure to inflate the door seal. Check the door bladder, the nitrogren pressure, and the pressure switch. Be sure there is 20-21 psi on RG2 and that the pressure switch turns off when the pressure reaches 17-18 psi.

HELP-2

Nitrogen Pres

There is insufficient pressure in the system nitrogen line. Check the nitrogen pressure switch (PSW1). It should be set to approximately 13 psi. Check the system line for leaks. Be sure that the pressure at RG1 is 23 psi dynamic. Check the Clean Coil thermostat and reset if necessary.

HELP-3

Door Open

The door is not completely closed. Check the door. If the door is properly aligned, check the micro-swtich actuating arm.

HELP-4

Index Failure

The unit is not able to index the rotor. Check the rotor positioner.

HELP-5

Excessive Speed

The rotor speed has exceeded 3400 RPM. Retry the cycle a few minutes. If the problem persists, there is a hardware problem. Call maintenance or VERTEQ for assistance.

 

11.0      Figures and Schematics

 

AMBIENT

TANK #1

DRAIN

 
       

Figure 1 – Quick Dump Rinse (QDR)                            Figure 2 –  Room Temperature Bath Timer Controller


Figure 3 – Hot Bath Temperature Controller


 

              

Figure 4 – Main System Power/Alarm Controller

 

Figure 5 – Photohelic Differential Pressure Gauge

12.0   Appendix


Sink 7

 

Sink 7

MPC-100 Temperature Controller Codes

 

MICROKLEEN Rinse Codes

Timer

Temperature (ºC)

 

Cycles

Cycles

LED Displays

 

LED Displays

Cr

11

 

CY

2

Pb

1.0

 

FP

45

rE

1.0

 

dP

5

rA

0.0

 

Sd

2

OF

0.0

 

Ad

0

AC1

00

 

n2

n

AC2

00

 

Ac

0

PS

Left bath: 60.0          Right bath: 160.0

 

PC

5

dr

Left bath: 60.0          Right bath: 74.5

 

Pn

1

 

 

 

nb

0

Temperature (ºC)

Timer

 

SL

1